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picture1_Best Flyer Templates Free Download 11467 | Data Qualifiers Table Basic Four Tests | Sample Application


 199x       Filetype XLS       File size 0.04 MB       Source: dnr.wisconsin.gov


File: Best Flyer Templates Free Download 11467 | Data Qualifiers Table Basic Four Tests | Sample Application
corrective action and dmr qualification table for wwtp basic four tests corrective test action must dmr must example of how best to qualify this data on the dmr be taken ...

icon picture XLS Filetype Excel XLS | Posted on 05 Jul 2022 | 3 years ago
Partial file snippet.
         Corrective Action and DMR Qualification Table for WWTP Basic Four Tests [5.5.11]
                                                                   Corrective 
                               Test                               Action Must      DMR Must               Example of How Best to qualify this data on the DMR
                                                                  Be Taken and  Be Qualified
                                                                  Documented
                          For All Tests                           For All Tests   For All Tests                                 For All Tests
    Your sample acceptance policy must indicate under what             Yes
 conditions samples received will require the data be qualified.   contact client      Yes        Results [indicate test affected] from sample date mm/dd/yy were received 
                  If these conditions exist then                                                                             in "state condition"
    Samples received with improper chemical or temperature             Yes
  preservation, beyond holding time, inappropriate containers,    contact client       Yes        Results [indicate test affected] from sample date mm/dd/yy were received 
                       insufficient volume                                                                                   in "state condition"
              QCS (Quarterly Blind Standard) failed                    Yes             No                                            NA
                        PT standard failed                             Yes             No                                            NA
                            IDC failed                                 Yes             No                                            NA
        LOD study failed (not applicable to TSS or BOD)                Yes             No                                            NA
                               TSS                                     TSS            TSS                                           TSS
          Analytical balance - weight verification failed              Yes             No                                            NA
             Insufficient residue captured (< 1.0 mg)                  Yes             No                                            NA
             Too much residue captured (> 200 mg)                      Yes             No                                            NA
                  Quarterly Re-dry study failed                        Yes             No                                            NA
                              BOD                                     BOD             BOD                                           BOD
                                                                                                  Samples should never be analyzed with a failing DO meter calibration.  In 
                   DO meter calibration failed                         Yes             Yes          the rare rare event that this must happen the data should be qualified 
                                                                                                                 indicating what sample dates were affected
                Blank depleted 0.25 mg/L or more                       Yes             Yes        The BOD blank associated with sample dates mm/dd/yy [list all dates that 
                                                                                                                                apply] failed.
                           GGA failed                                  Yes             Yes        The BOD GGA std associated with sample dates mm/dd/yy [list all dates 
                                                                                                                        that apply] failed high or low.
            None of the seed control dilutions passed                  Yes             No                                            NA
                None of the BOD dilutions passed                       Yes             No                                            NA
    Samples were supersaturated (> 0.4 TDO or > 9.0 mg/L)              Yes             No                                            NA
                             NH3-N                                   NH3-N           NH3-N                                         NH3-N
                                                                                                  Samples should never be analyzed using a failed initial calibration.  The 
                      Initial calibration failed                       Yes             Yes         calibration issue is to be fixed and samples reanalyzed.  In the rare rare 
                                                                                                  event that this must happen the data should be qualified indicating what 
                                                                                                       sample dates were affected by the failed calibration for NH3-N
                                                                                                  Samples should never be reported using a failed CCV.  The CCV issue is 
   CCV failed (use when more than 20 samples analyzed in a             Yes             Yes        to be fixed and samples reanalyzed.  In the rare rare event that this must 
                              batch)                                                                happen the data must be qualified indicating what sample dates were 
                                                                                                                    affected by the failed CCV for NH3-N
                       Method blank failed                             Yes             Yes       NH3-N sample dates mm/dd/yy [list all dates that apply] were reported with 
                                                                                                                            a failed method blank
                            LCS failed                                 Yes             Yes       NH3-N sample dates mm/dd/yy [list all dates that apply] were reported with 
                                                                                                                                a failed LCS
    Results reported when the response was higher than the             Yes             Yes       NH3-N sample dates mm/dd/yy [list all dates that apply] were reported with 
                        calibration range                                                                      a result that was not within the calibration range
                               TP                                       TP             TP                                            TP
                                                                                                  Samples should never be analyzed using a failed initial calibration.  The 
                      Initial calibration failed                       Yes             Yes         calibration issue is to be fixed and samples reanalyzed.  In the rare rare 
                                                                                                  event that this must happen the data should be qualified indicating what 
                                                                                                         sample dates were affected by the failed calibration for TP
                                                                                                  Samples should never be reported using a failed ICV.  The ICV issue is to 
                            ICV failed                                 Yes             Yes         be fixed and samples reanalyzed.  In the rare rare event that this must 
                                                                                                    happen the data must be qualified indicating what sample dates were 
                                                                                                                       affected by the failed ICV for TP
                                                                                                  Samples should never be reported using a failed CCV.  The CCV issue is 
                           CCV failed                                  Yes             Yes        to be fixed and samples reanalyzed.  In the rare rare event that this must 
                                                                                                    happen the data must be qualified indicating what sample dates were 
                                                                                                                      affected by the failed CCV for TP
                       Method blank failed                             Yes             Yes        TP sample dates mm/dd/yy [list all dates that apply] were reported with a 
                                                                                                                             failed method blank
                            LCS failed                                 Yes             Yes        TP sample dates mm/dd/yy [list all dates that apply] were reported with a 
                                                                                                                                 failed LCS
    Results reported when the response was higher than the             Yes             Yes        TP sample dates mm/dd/yy [list all dates that apply] were reported with a 
                        calibration range                                                                      result that was not within the calibration range
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...Corrective action and dmr qualification table for wwtp basic four tests test must example of how best to qualify this data on the be taken qualified documented all your sample acceptance policy indicate under what yes conditions samples received will require contact client results from date mmddyy were if these exist then in state condition with improper chemical or temperature preservation beyond holding time inappropriate containers insufficient volume qcs quarterly blind standard failed no na pt idc lod study not applicable tss bod analytical balance weight verification residue captured mg too much redry should never analyzed a failing do meter calibration rare event that happen indicating dates affected blank depleted mgl more associated gga std high low none seed control dilutions passed supersaturated tdo nhn using initial issue is fixed reanalyzed by reported ccv use when than batch method lcs response was higher range result within tp icv...

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